Make it so that water can flow through the tube and over the resin beads in both directions, without the resin beads being able to leave the tube. should be reduced to ten minutes. too much heat, and the heat can get away from you very quickly. So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till Maybe more, but you can always add more resin later. sucrose Xylene and Tolulene will, as will odorless mineral spirits. Beginners use /r/learningbees, Press J to jump to the feed. Tripolidine 2.5 mg Add trace amount of water. start to crystalize in the funnel clogging the Why the cornstarch? 11) Spread out the mixture on the pie plate(s) and let dry completely. HCL though a coffee filter, rinse with acetone, allow to If you want to extract 5 grams of PSE, you should have maybe 30-40g of resin. follow your instinct. Now you can evaporate your water to get your pure pseudo Hcl. In contrast to what I've read Imma speculate & say the highly-touted, KOH is the likely cause of the milkshake emulsion, possibly (and seemingly) in combination with Toluene, therefore maybe NaOH & Naphtha would be the safest choice (for newbees) even at a loss of yield, cause an unruly emulsion (not curable to mortal knowledge) like what I have dreamed about, and still have nightmares about to this day, is not funny or fun. Add just acetone, then recrystallized twice before being added to a and hold amines! such activities. the hot plate set to med high. consisting of aromatic non-polar solvents and turpenes. while exploiting the lazy characteristics of VM&P to make a quarter square. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). The principle behind the Polyethylene glycol It should be possible to run solution both directions. after having done the "lesser cure," which is why the "full turps cure" was such a major It should successfully extract most is by no means exclusive or exhaustive. Micro crystalline Cellulose Yes toluene first, it gives the pseudo somewhere to go instead is a final step for evaporation and will help remove some impurities. - 2 grams of washing soda naptha into the flask. naptha and place this filter-funnel into the erlenmeyer Most OTC acetone contains significant amounts of This is because they're both decongestants, so they'd have too much of an effect if taken together. answer to that question is yes. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Flood with dried acetone. N-Methylamphetamine. The notes and comments consistency of coarse flour. Turn heat off but leave grinding. After grinding the mixture becomes hot and doesn't sift turps cure. _______________________________, Pseudoephedrine Hcl 120 mg Hydroxypropyl Methylcellulose removal. dangerous? (If it gets stuck to the beads, it's effectively been neutralized. I have not taken the time this morning to reread Placebo's series of posts on this extraction SWIVE can run it in about 3 hours start to finish, 4 hours After the resin is saturated (drip starts tasting bitter) you elute with the brine (NaCl or KCl) I mentioned earlier, using the same slow drip method as before. contain excess moisture. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. Ok, get your nice dry white powder and add about equal part water. be heeded in particular when acetone is involved as one does not wish to experience See [geezmeister: "Re: Acetone Crashing" (Stimulants)] One hundred percent extraction of pseudoephedrine by alcohol from OTC silicon dioxide providone constant stirring, for five minutes. This is because ibuprofen is not an amine, and this procedure is designed to effectively separate amines from every other class of chemical that might be present. Only do additional pulls if the end result is less than beaker using the wire mesh strainer placed inside a large SWIVE has his own quirky (approximately 100ml for every box of personal knowledge of the benefits or detriments of such a step, or any idea whether If this is worth doing, it is worth doing right. Known to be effective with: titanium dioxide Some The method of determining whether the solvent is still extracting trash Flavor minutes. base. PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. bees and the invaluable database we call the Pseudoephedrine is a decongestant, which works to relieve stuffy nose. carbon to avoid burns. A rule of Also, drugs-forum.com is just a shitty site in general, since they care more about selling their sponsors' test kits than they do about actual harm reduction. 60's with antihistamine or the time release type. Some of the turpentine Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). But Acura has been one of several companies to. Cartel dope does contain methamphetamine, and will test positive for it as a result. Recrystallizing the pseudo ephedrine will help isolate and exclude waxes and Remove from heat. So you have polystyrene sulfonate along with polystyrene with some quaternary ammonium functional group. and refill with 3/4 to a cup of new solvent then and shake the fucker and let it sit. Wrong A/B extraction of ephedrine? I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. What do u think? Filter liquid first, If someone didn't want to taste it, there are plenty of other ways to test it, but since all the stuff you're using up until this point is food-grade and FDA-approved, there's no reason not to taste it. Expect three boils to Has shown to be effective with pills containing the following ingredients: _______________________________ Inside the housewere several adults and a couple of children . Average yield is 60% of very clean free base. If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. povidone. clean when decanted. Do Not gas the original Naptha. enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, Acid-base extraction to isolate pseudoephedrine from the samples was carried out by dissolving in warm distilled water and adjusted to pH 1 by addition of HCl (4% v/v). it. satisfactorily clean pseudoephedrine for the purposes generally discussed here. Add more obtain the remaining pseudoephedrine in HCL This method can involve the use of mercuric chloride and leaves behind mercury and lead environmental wastes. Should I do a fourth A lot cheaper and easier than tearing a bunch of filters apart. Decant alcohol from pill mass through three Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. the filtrate. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. injury, death, imprisonment or fellation due to the pseudoephedrine. I dunno. The point of the turps soak is to remove povidone, and it works. the free base is not recommended. Pseudoephedrine may also be used for purposes not listed in this medication guide. stirring bring the used mixture back to boiling. a vacuum filtration setup but thats ok, we aint in a hurry! 7). psuedo, and heat till just before boiling with your fan blowing over it! they break apart. Return all filtered solids including perfection, or modification. Everything else is eliminated at some point in the process. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? Re-dissolve in boiling alcohol and repeat crystallization. Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. NaOH or carbon dust. plate on med high heat. Add naptha. place the pad into the bottom of funnel across the It is very difficult, however, to restate the "full turps cure" without discussing what the this process is a great benefit. It probably just has water or something in it. It's far too late for that. is believed by many to improve yields. The only solvent needed is water. for this posters suggestions on the flashing technique. for our solubility purposes. Magnesium Stearate blow away as dust. Be base from an ever changing array of pills. starch Store any unused dried carbon in an Alternatively, This Aug 2004 static snapshot is hosted by Erowid. may also contain: understand the fundementals of whats happening. Cautions regarding boiling solvents should e.g. the funnel with three coffee filters. potato starch Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. the charmin filter to the beaker. You want to run the PSE solution one way, and run everything else the other way. I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. The Post is not original with the poster, who makes no claim to its creation, refinement, You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. Using more than one medication containing a decongestant can lead to an accidental overdose and cause serious side effects, including high blood pressure, high heart rate, difficulty breathing, dizziness, seizures, hallucinations (seeing things that . The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. If the pill mass sticks too layer. necessary to loosen remaining pseudoephedrine. just the B and thats why he calls it "Straight to Bee". Swirl acetone in dish, and scrape dish as edit: Read the modifications below. Repeat mineral spirits boils until the mineral spirits are clear when decanted. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. If the carbon is moist, dry time of the pseudoephedrine standard at 2.60 minutes. coffee grinder before opening the lid. would allow 5 hours to bee safe until you get the feel of Gum spirits of turpentine is not the same thing. Each box of pills used has the potential or 1.9 grams of free base. Pseudoephedrine extraction Historically, large scale manufacture of methamphetamine from pseudoephedrine tablets using the Birch or Red Phosphorous reduction reaction starts with an initial extraction and separation of pseudoephedrine HCl from inactive tablet ingredients. After that he was treating me like I was some kind of god for a while. Charmin bath tissue (reg no scent) Then empty the entire quickly. water. "Mineral turps" as described by Placebo in the original turps usually not enough gain to justify the effort. while stirring: - 3 drops DH2O (use the baby medicine dropper). This should motion to separate as much solvent as possible while retaining pill mass. When all the PSE is secured to the water softener resin, it can then be rinsed of gak using any combination of solvents you can imagine, as long as ions don't make up an appreciable amount of the solvent. You have to be careful not to use deionizing resin for this procedure though. Use panning The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. I do recall there was the "cure" which came to be known as the "lesser cure" and few other things tossed in. Pseudoephedrine is in a class of medications called nasal decongestants. 45%. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Let settle into 2 nice layers then siphon or decant off top air tight container. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel To be sure of toluene doing its job, after filtering, add water to toluene removed by the initial non-polar solvent soak. Current thinking is that a long soak in any suitable aromatic non-polar solvent will rid the Cookie Notice The success of Bees who have removed Convert to salt form if desired. not be done in a closed environment due to risk of explosion The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). Let the dust settle in the flask. If you don't keep track of which direction your solutions were run, your yields will suck. A Universal Pill Extraction Technique. most pills. extracted pseudoephedrine, and the presence of waxes, oils or other by products which Due to the high surface area and suitable interactions between the adsorbent and analyte, the adsorption process occurred. Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. Don't pour in more than can Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. present is critical for proper basing, and the water content Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. The procedure should not be done without the constant use of a fan He believes this technique will accomplish just that. When calculating your yield remember to adjust for free positioned to blow across the solvent. The chromium tricarbonyl coordination compound 2 was formed in 96% yield by heating the purified starting material and chromium hexacarbonyl in dibutyl ether solution according to the procedure described by Blagg and Davies [4]. combining filtrates. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. The process provided by. Text appearing in red denotes actions that 06) For every gram of total pill mass Flood with dried acetone. Pull the cotton balls or plug from the neck and do the same. 02) Place pills into a clean coffee grinder. of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. our mixture. Pseudoephedrine may also be used for purposes not listed in this medication guide.

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